Effects of print orientation and artificial aging on the flexural strength and flexural modulus of 3D printed restorative resin materials

Mudhaffer, Shaymaa, Haider, Julfikar ORCID: https://orcid.org/0000-0001-7010-8285, Satterthwaite, Julian and Silikas, Nick (2024) Effects of print orientation and artificial aging on the flexural strength and flexural modulus of 3D printed restorative resin materials. The Journal of Prosthetic Dentistry. ISSN 0022-3913

Preview

Published Version Available under License Creative Commons Attribution. Download (9MB) | Preview

Abstract

Statement of problem The integration of computer-aided design and computer-aided manufacture (CAD-CAM) technology has revolutionized restorative dentistry, offering both additive and subtractive manufacturing methods. Despite extensive research on 3-dimensionally (3D) printed materials, uncertainties remain regarding the impact of print orientation on their mechanical properties, especially for definitive resin materials, necessitating further investigation to ensure clinical efficacy. Purpose The purpose of this in vitro study was to investigate the influence of print orientation and artificial aging on the flexural strength (FS) and flexural modulus (FM) of 3D printed resin materials indicated for definitive and interim restorations. Material and methods Specimens (2×2×25 mm) were additively manufactured in 3 orientations (0, 45, and 90 degrees) using five 3D printed resins: VarseoSmile Crownplus (VCP), Crowntec (CT), Nextdent C&B MFH (ND), Dima C&B temp (DT), and GC temp print (GC). A DLP 3D printer (ASIGA MAX UV) was used with postprocessing parameters as per the manufacturer recommendations. FS and FM were tested after storage in distilled water (DW) and artificial saliva (AS) for 24 hours, 1 month, and 3 months at 37 °C. Additional 2×2×16-mm specimens printed at 90 degrees were compared with the milled materials Lava Ultimate (LU) and Telio CAD (TC) after 24 hours of storage in AS at 37 °C (n=10). Measurements were conducted using a universal testing machine (Z020; Zwick/Roell) following the International Organization for Standardization (ISO) 4049 standard. Multiple way ANOVA, 1-way ANOVA, and Tukey HSD post hoc tests (α=.05) were used to analyze the data. Results Print orientation significantly influenced the FS and FM of 3D printed resin materials, with the 90-degree orientation exhibiting superior mechanical properties (P<.05). Definitive resins (CT and VCP) exhibited higher FS and FM compared with interim resins (ND, DT, GC) at all time points (P<.001). LU had significantly higher FS and FM compared with other resins (P<.001), while TC had similar FS to definitive 3D printed resins. Aging time and media influenced FS and FM, with varying effects observed across different materials and time points. Strong positive correlations were found between filler weight and both FS (r=.83, P=.019) and FM. All materials met the minimum FS requirement of 80 MPa (ISO 4049) when printed at 90 degrees. Conclusions The 90-degree orientation produced specimens with higher FS than 0- and 45-degree orientations. CT recommended for definitive restorations displayed higher FS compared with VCP and those intended for interim use after 3 months of aging. LU exhibited higher FS and FM than 3D printed resins, while TC had similar FS and FM to the latter. Aging effects on 3D printed resins were minimal and were material specific.